반응 #52585

반응 방정식

5-Fluoroisatin

→

title compound

5-Fluoro-2-oxindole

용매

hydrazine hydrate

—

ice water

반응 조건

후처리

1. 1
   온도refluxed for 1.0 hr
2. 2
   기타The reaction mixtures
3. 3
   여과The precipitate was then filtered
4. 4
   세척washed with water
5. 5
   기타dried in a vacuum oven

실험 절차

5-Fluoroisatin (8.2 g) was dissolved in 50 mL of hydrazine hydrate and refluxed for 1.0 hr. The reaction mixtures were then poured in ice water. The precipitate was then filtered, washed with water and dried in a vacuum oven to afford the title compound.

출처