반응 #523831

반응 방정식

4-trifluoromethoxybenzoyl chloride

cystamine dihydrochloride

sodium hydroxide

→

N,N'-(Dithiodiethylene)bis(4-trifluoromethoxybenzamide)

용매

ethylene dichloride

반응 조건

후처리

1. 1
   기타, was prepared as in Example 1 using 33.6 g
2. 2
   기타of ethylene dichloride and recrystallization from acetonitrile using

실험 절차

m.p. 150°-151° C., 14.5 g., was prepared as in Example 1 using 33.6 g. of 4-trifluoromethoxybenzoyl chloride in 100 ml. of ethylene dichloride, 11.3 g. of cystamine dihydrochloride, 300 ml. of 10% sodium hydroxide solution, 400 ml. of ethylene dichloride and recrystallization from acetonitrile using decolorizing charcoal.

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