반응 #5223

ord-dcadfe0e1eca4e47a8b88dad58fe8309

용매

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    workup.STIRRINGThereafter, the mixture was stirred at room temperature for 19 hours

실험 절차

2-Aminoethanol (13.76 g, 225.3 mmol) was dissolved in CHCl3 (750 ml). To the solution was added dropwise palmitoyl chloride (15.48 g, 56.3 mmol) with stirring under ice cooling. Thereafter, the mixture was stirred at room temperature for 19 hours.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05243035uspto-grants-1993_09