반응 #521530

ord-b42fea7601154edc9313ca94105ec94a

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타The solvent is then evaporated after which the 2-(4-cyclohexylphenyl)imino-hexahydropyrimidine zinc chloride complex
  2. 2
    기타is obtained

실험 절차

10.3 g of 2-(4-cyclohexylphenyl)imino-hexahydropyrimidine are dissolved in 150 ml of warm acetonitrile. To this solution is added a warm solution of 2.7 g of zinc-chloride in acetonitrile. The solvent is then evaporated after which the 2-(4-cyclohexylphenyl)imino-hexahydropyrimidine zinc chloride complex is obtained. The complex is characterized by the I.R.-spectrum.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04396617uspto-grants-1983_08