반응 #521490

ord-241ae64773394f13b9e7dc796654469b

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타A white precipitate formed immediately
  2. 2
    여과The mixture was filtered
  3. 3
    기타air dried

실험 절차

To a solution of 5.5 g (0.03 mole) of anhydrous cadmium chloride in 120 ml of ethanol was added a solution of 4.5 g (0.03 mole) of 5-chloro-2-methyl-3-isothiazolone in 25 ml of ethanol. A white precipitate formed immediately. The mixture was filtered and air dried to yield 10.0 g (100%) of product, m.p. >250° C.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04396413uspto-grants-1983_08