반응 #520803
ord-e0e89c22dafd435b9479628bf8426f6b
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반응물
시약
반응 조건
상세 조건
See reaction.notes.procedure_details.
실험 절차
Following the general method described in example 234, 3-(methylthio)aniline was reacted with triethyl orthoformate, ethyl nitroacetate and acetic acid followed by treatment with triethyl orthoformate, iron and acetic acid and subsequent alkaline hydrolysis. The title compound was obtained as a grey crystalline solid. Mp. 190-192° C. (H2O/dioxane), MS: m/e=234 (M+).