반응 #52043

ord-36905fa681b1473c9ca583a21c17dc15

용매

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    세척After washing
  2. 2
    기타phase separation

실험 절차

4-chloro-3-nitro-quinoline is reacted with isobutyl amine in the presence of triethylamine (TEA) at between −10 and +15° C. in toluene, while excluding moisture. After washing and phase separation, the organic solution is ready for the next step.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US06852861B2uspto-grants-2005_02