반응 #518095

ord-12e6d8d90c484058b50236fc8c75e009

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타The same reaction

실험 절차

The same reaction and after-treatment using 81.1 g (0.46 mole) of p-tert-butoxystyrene and 4.6 g (0.04 mole) of styrene as described in Production Example 4-(1) were conducted to give 80.5 g of poly(p-tert-butoxystyrene/styrene) as white powders. Then, the polymer was subjected to the same reaction and after-treatment as described in Production Example 9-(1) to give 44.0 g of poly(p-hydroxystyrene/styrene) as white powders. A ratio of p-hydroxystyrene unit and styrene unit was about 92:8 by 1HNMR. Mw: about 15500, Mw/Mn: 1.08 (GPC method: polystyrene as standard).

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US06656660B1uspto-grants-2003_12