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5-Isopropyl-2-nitro-4-thiocyanato-phenylamine

hydrogen

→

4-Isopropyl-5-thiocyanato-benzene-1,2-diamine

용매

THF

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실험 절차

5-Isopropyl-2-nitro-4-thiocyanato-phenylamine (prepared in Example QQ-1; 7.83 g, 33 mmol) was hydrogenated using Raney nickel (2 g) and THF (100 mL) in the presence of hydrogen (50 psi) as described in General Method 3. MS(APCI): 208(M+H).

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