반응 #51737

반응 방정식

5-tert-butyl-6-thiocyanato-benzothiazol-2-yl-amine

dithiothreitol

phosphate

→

title compound

2-Amino-5-tert-butyl-benzothiazole-6-thiol

용매

EtOH

반응 조건

실험 절차

The title compound was prepared according to General Method 14 using 5-tert-butyl-6-thiocyanato-benzothiazol-2-yl-amine (Example L-1; 8 g, 30 mmol), dithiothreitol (18.7 g, 121 mmol), EtOH (200 mL), and phosphate buffer (50 mL). MS (APCI): 239 (M+H).

출처