반응 #51463

ord-d6bb0716c7774a2aab46372d086f0417

용매

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타all volatiles were removed under reduced pressure

실험 절차

N-Boc sarcosine piperonylamide (500 mg, 1.54 mmol) in methanol (10 mL) was treated with acetyl chloride (1 mL). After 45 minutes, all volatiles were removed under reduced pressure to yield sarcosine piperonyl amide hydrochloride (395 mg, quant.) as a sticky solid.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US06849739B2uspto-grants-2005_02