반응 #51444
ord-bc89b3c8c1c4439892dd33fbdfc6e764
반응 방정식
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타the solvent is evaporated under vacuum
실험 절차
An amount of 3.47 g (0.015 mole) of 5-nitro-3-chloro-2,4-difluorobenzoic acid and 2.03 g (0.016 mole) of oxalyl chloride are dissolved in 15 ml of dichloromethane then two drops of DMF are added. The reaction is stirred for 14 hours then the solvent is evaporated under vacuum to afford the desired product.