반응 #514222

반응 방정식

Methyl 3-(2-aminoanilino)-2,5-dihydrothiophene-4-carboxylate

norbornadiene

norbornylene

→

Methyl 3-(2-aminoanilino)-thiophene-4-carboxylate

용매

cyclohexene

반응 조건

후처리

1. 1
   온도the reaction was heated
2. 2
   온도at reflux

실험 절차

Methyl 3-(2-aminoanilino)-2,5-dihydrothiophene-4-carboxylate (2.5 g, 0.001 mol) was added to a flask containing palladium on charcoal catalyst (5%, 200 mg) in cyclohexene (or norbornadiene or norbornylene) (50 ml and the reaction was heated at reflux with stirring for 4 hours, the reaction being followed by t.l.c.

출처