반응 #5142

ord-a6e9045e32c049c09013afb37b5d1d71

반응 방정식

Cc1cc(C)cc(Br)c1
5-bromo-m-xylene
C[Si](C)(C)Cl
chlorotrimethylsilane
→
Cc1cc(C)cc([Si](C)(C)C)c1
5-Trimethylsilyl-m-xylene

반응물

Cc1cc(C)cc(Br)c1
5-bromo-m-xylene
C[Si](C)(C)Cl
chlorotrimethylsilane

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타afforded TSIX
  2. 2
    기타The yield

실험 절차

In the same manner as described in preparation 1, 5-bromo-m-xylene was allowed to react with chlorotrimethylsilane, and afforded TSIX. The yield and properties of product are summarized in Table 1.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05243010uspto-grants-1993_09