반응 #51407

반응 방정식

cinnamoyl chloride

aniline

→

4-Phenyl-3,4-dihydrocarbostyril

반응 조건

후처리

1. 1
   기타The title compound was purified by flash chromatography
2. 2
   세척eluting with CH2Cl2/EtOAc (4:1)

실험 절차

4-Phenyl-3,4-dihydrocarbostyril (CAS# 4888-33-9) was prepared in two steps using the procedure described by Conley, R. T.; Knopka. W. N. J. Org. Chem. 1964, 29, 496-497. The starting materials for this preparation were cinnamoyl chloride (Aldrich) and aniline (Aldrich). The title compound was purified by flash chromatography eluting with CH2Cl2/EtOAc (4:1).

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