반응 #51393

반응 방정식

cyclopentylacetic acid

L-alanine iso-butyl ester hydrochloride

→

title compound

N-(cyclopentylacetyl)-L-alanine iso-butyl ester

반응 조건

후처리

1. 1
   기타The reaction was monitored by tlc on silica gel (Rf=0.37 in 1:3 EtOAc:hexane) and purification
2. 2
   추출was by extraction with Et2O

실험 절차

Following General Procedure BB above, and using cyclopentylacetic acid (Aldrich) and L-alanine iso-butyl ester hydrochloride (from Example BB above), the title compound was prepared as a solid having a melting point of 62° C.-64° C. The reaction was monitored by tlc on silica gel (Rf=0.37 in 1:3 EtOAc:hexane) and purification was by extraction with Et2O followed by washes with aqueous K2CO3 and aqueous HCl.

출처