반응 #51310

반응 방정식

3,4-dichloroaniline

n-propyl pyruvate

→

title compound

N-(3,4-dichlorophenyl)alanine n-propyl ester

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후처리

1. 1
   기타The reaction was monitored by tlc on silica gel (Rf=0.5 in 25% EtOAc/hexanes) and purification

실험 절차

Following General Procedure AA above and using 3,4-dichloroaniline (Aldrich) and n-propyl pyruvate (prepared by following General Procedure AO above using n-propanol in place of iso-butanol), the title compound was prepared as an oil. The reaction was monitored by tlc on silica gel (Rf=0.5 in 25% EtOAc/hexanes) and purification was by preparative plate chromatography (silica gel using 25% EtOAc/hexanes as the eluant).

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