반응 #51287

ord-67b0e0ea560741a29465b3e78fa61211

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타Purification
  2. 2
    기타was by recrystallization from ethyl acetate/hexanes

실험 절차

Following General Procedure II-E above using cyclopentylacetic acid (Aldrich) and L-alanine methyl ester hydrochloride (Sigma), the title compound was prepared as a solid having a melting point of 43-46° C. Purification was by recrystallization from ethyl acetate/hexanes.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US06849650B2uspto-grants-2005_02