반응 #5127
ord-4bb73f6b08114a6bb1231cd70986f4d3
반응 방정식
반응 조건
상세 조건
See reaction.notes.procedure_details.
실험 절차
10.2 g (0.011 mol) of 1,17-biscyclohexylguanidino-9-azaheptadecane dihydroiodide in 150 ml of methanol/water (1:1) were filtered through a column containing 250 g of ion exchanger (OH- form). The free guanidine base obtained after working up was dissolved in methanol and converted into the triacetate with excess glacial acetic acid.