반응 #51260

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Ethyl 1-{4-[(aminothio)peroxy]phenyl}-8-nitro-4,5-dihydro-1H-benzo[g]indazole-3-carboxylate

3-(aminosulfonamido)-phenylhydrazine

→

Ethyl 1-[3-(aminosulfonyl)phenyl]-8-nitro-4,5-dihydro-1H-benzo[g]indazole-3-carboxylate

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후처리

1. 1
   기타This compound was prepared

실험 절차

This compound was prepared using the same procedures for Ethyl 1-{4-[(aminothio)peroxy]phenyl}-8-nitro-4,5-dihydro-1H-benzo[g]indazole-3-carboxylate of Example 2, where 3-(aminosulfonamido)-phenylhydrazine was used in place of 4-(aminosulfonamido)-phenylhydrazine. Its structure was confirmed by 1H NMR and MS (443, M+1). C20H18N4O6S, Calc.: C: 54.29; H: 4.10; N: 12.66; Found, C: 54.27; H: 4.09; N: 12.55.

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