반응 #511558

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18m

2-Bromo-4-fluoro-1-(methoxymethoxymethyl)benzene

19b

1,3-Dihydro-5-fluoro-1-hydroxy-2,1-benzoxaborole

→

1,3-Dihydro-6-fluoro-1-hydroxy-2,1-benzoxaborole

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실험 절차

This compound was made from 18m in the same manner as compound 19b: 1H NMR (300 MHz, DMSO-d6) δ (ppm) 4.95 (s, 2H), 7.29 (td, J=9.0, 2.7 Hz, 1H), 7.41-7.46 (m, 2H), 9.29 (s, 1H); ESI-MS m/z 151 (M−H)−; HPLC purity 100%; Anal (C7H6BFO2) C, H.

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