반응 #511557

반응 방정식

18h

2-Bromo-1,5-bis(methoxymethoxymethyl)benzene

19b

1,3-Dihydro-5-fluoro-1-hydroxy-2,1-benzoxaborole

→

1,3-Dihydro-1-hydroxy-5-hydroxymethyl-2,1-benzoxaborole

반응 조건

실험 절차

This compound was made from 18h in the same manner as compound 19b: mp 124-128° C.; 1H NMR (300 MHz, DMSO-d6) δ (ppm) 4.53 (d, 2H), 4.94 (s, 2H), 5.24 (t, 1H), 7.26 (d, 1H), 7.33 (s, 1H), 7.64 (d, 1H), 9.08 (s, 1H); ESI-MS m/z 163 (M−H)−; HPLC purity 100%.

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