반응 #511556

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18g

2-Bromo-5-methoxy-1-(methoxymethoxymethyl)benzene

19b

1,3-Dihydro-5-fluoro-1-hydroxy-2,1-benzoxaborole

→

1,3-Dihydro-1-hydroxy-5-methoxy-2,1-benzoxaborole

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실험 절차

This compound was made from 18g in the same manner as compound 19b: mp 102-104° C.; 1H NMR (300 MHz, DMSO-d6) δ (ppm) 3.77 (s,3H), 4.91 (s, 2H), 6.88 (d, J=8.1 Hz, 1H), 6.94 (s, 1H), 7.60 (d, J=8.1 Hz, 1H), 8.95 (s, 1H); ESI-MS m/z 163 (M−H)−; HPLC purity 100%; Anal (C8HgBO3) C, H.

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