반응 #511545

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2-bromo-5-methylbenzoic acid

18d

2-Bromo-5-chloro-1-(methoxymethoxymethyl)benzene

→

4-Bromo-3-(methoxymethoxymethyl)toluene

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실험 절차

This compound was made from 2-bromo-5-methylbenzoic acid in the same manner as compound 18d: 1H NMR (300 MHz, DMSO-d6) δ (ppm) 2.27 (s, 3H), 3.30 (s, 3H), 4.51 (s, 2H), 4.68 (s, 2H), 7.05 (dd, J=7.9, 2.3 Hz, 1H), 7.30 (d, J=1.5 Hz, 1H), 7.46 (d, J=8.2 Hz, 1H).

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