반응 #51076

반응 방정식

2-amino-5-nitropyridine

2,6-dimethylphenyl isocyanide

3-hydroxybenzaldehyde

→

Compound ( 12 )

3-[3-(2,6-dimethylphenylamino)-6-nitroimidazo[1,2-a]pyridin-2-yl]-phenol

용매

perchloric acid

반응 조건

실험 절차

Compound (12) was prepared according to the general synthesis instructions from 1.0 ml of 2-amino-5-nitropyridine solution (0.1 M, DCM), 0.575 ml of 2,6-dimethylphenyl isocyanide solution (0.2 M, DCM), 0.500 ml of 3-hydroxybenzaldehyde solution (0.3 M, DCM), and 10 μl of perchloric acid (w=20%).

출처