반응 #50873
ord-82aa24b70650476f8934154e035255ed
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1여과The solid title compound was collected by filtration
실험 절차
A solution of isophthalaldehyde (4.0 g) and 7-chloroquinaldine (5.39 g) in acetic anhydride was heated at 125° in an oil bath for 48 hours. The reaction was cooled to room temperature, diluted with ether (30 mL) and the resulting suspension was stirred vigorously. The solid title compound was collected by filtration and was used as such in the next step.