반응 #508701

ord-657664ae31724dcea29b0f6ece69caaa

반응 방정식

CCCCCCCCCCCC(=O)OCC(O)CO
glycerol monolaurate
CCCCCCCCCCCCCCCCO
cetyl alcohol
CCCCCCCCCCCC(=O)OCC(O)CO
glycerol monolaurate
CCCCCCCCCCCCCCCCO
cetyl alcohol
CCCCCCCCCCCCCCCCCC(=O)O
stearic acid
CCCCCCCCCC[N+](C)(C)CCCCCCCCCC.[Cl-]
DDAC
→
CCCCCCCCCCCCCCCCCC(=O)O.OCCN(CCO)CCO
Triethanolamine Stearate

반응물

CCCCCCCCCCCC(=O)OCC(O)CO
glycerol monolaurate
CCCCCCCCCCCCCCCCO
cetyl alcohol
CCCCCCCCCCCC(=O)OCC(O)CO
glycerol monolaurate
CCCCCCCCCCCCCCCCO
cetyl alcohol
CCCCCCCCCCCCCCCCCC(=O)O
stearic acid
CCCCCCCCCC[N+](C)(C)CCCCCCCCCC.[Cl-]
DDAC

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    workup.ADDITIONInstead of being added in the second step
  2. 2
    workup.ADDITIONwas added
  3. 3
    workup.ADDITIONafter the addition of TEA

실험 절차

Example 2A was repeated but for the sequence of addition of glycerol monolaurate and cetyl alcohol. Instead of being added in the second step, after the equimolar mixture of stearic acid and DDAC, the same amount of the glycerol monolaurate and cetyl alcohol added in Example 2 was added after the addition of TEA.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US08101163B2uspto-grants-2012_01