반응 #50708

반응 방정식

8-phenyloctyl chloride

sodium iodide

→

8-phenyloctyl iodide

용매

acetone

반응 조건

후처리

1. 1
   온도was heated
2. 2
   온도under reflux for 20 hours
3. 3
   기타Evaporated
4. 4
   workup.ADDITIONwater (20 ml) added
5. 5
   추출extracted with diethyl ether (20 ml)
6. 6
   기타The extracts were dried
7. 7
   여과filtered
8. 8
   기타evaporated to a pale yellow liquid (5.5 g)
9. 9
   workup.DISTILLATIONDistilled

실험 절차

A mixture of 8-phenyloctyl chloride (4.4 g), sodium iodide (5.34 g) and acetone (20 ml) was heated under reflux for 20 hours. Evaporated, water (20 ml) added and extracted with diethyl ether (20 ml). The extracts were dried, filtered and evaporated to a pale yellow liquid (5.5 g). Distilled to give 8-phenyloctyl iodide, b.p. 200° C. (air bath temperature) at 0.1 mBar.

출처