반응 #50373

ord-ff8a7db881944361986decaa997cade8

반응 방정식

COC(C(=O)O)=C(OC)c1ccccc1OC
trimethoxy cinnamic acid
OCC1CO1
glycidol
OCC(O)CO
glycerin
O=S(=O)(O)O
sulfuric acid
O=C(O)C=Cc1ccccc1
cinnamic acid

용매

반응 조건

온도
90°CELSIUS
상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    온도heating

실험 절차

4.35 g of trimethoxy cinnamic acid and 10 g of glycidol were dissolved in 5 ml of DMSO. The mixture was stirred and heated to 90° C. Catalystic amount of sulfuric acid was added, heating and agitation were carried out for 3.5 hours, and then the adduct of cinnamic acid and glycerin was obtained.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05426210uspto-grants-1995_06