반응 #50373
ord-ff8a7db881944361986decaa997cade8
반응 방정식
trimethoxy cinnamic acid
glycidol
glycerin
sulfuric acid
→
cinnamic acid
용매
반응 조건
온도
90°CELSIUS
상세 조건
See reaction.notes.procedure_details.
후처리
- 1온도heating
실험 절차
4.35 g of trimethoxy cinnamic acid and 10 g of glycidol were dissolved in 5 ml of DMSO. The mixture was stirred and heated to 90° C. Catalystic amount of sulfuric acid was added, heating and agitation were carried out for 3.5 hours, and then the adduct of cinnamic acid and glycerin was obtained.