반응 #50367
ord-9fd1cb87e984445880ac895829b5f575
반응 방정식
sodium hydroxide
p-hydroxy cinnamic acid
glycidol
sulfuric acid
→
cinnamic acid
반응 조건
온도
90°CELSIUS
상세 조건
See reaction.notes.procedure_details.
후처리
- 1온도heating
실험 절차
17.4 g of p-hydroxy cinnamic acid and 40.0 g of glycidol were dissolved in 20 ml of DMSO, and catalytic amount of sulfuric acid was added. The solution was heated to 90° C. and then heating and agitation was carried out for 3 hours, neutralized by adding sodium hydroxide and then adduct of cinnamic acid and glycerin was obtained.