반응 #50366

ord-12a47bbc2fa647d09b787ad23f92c3fb

반응 방정식

OCC1CO1
glycidol
OCC(O)CO
glycerin
O=C(O)C=Cc1ccc(O)cc1
p-hydroxy cinnamic acid
CCOCC.FB(F)F
boron trifluoride ethyl ether
O=C(O)C=Cc1ccccc1
cinnamic acid

용매

반응 조건

온도
90°CELSIUS
상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    온도heating

실험 절차

8.719 g of p-hydroxy cinnamic acid was dissolved in 10 ml of DMSO, and 19.7 g of glycidol was added. The mixture was stirred and heated to 90° C. Catalystic amount of boron trifluoride ethyl ether was added, heating and agitation was carried out for 2 hours and then the adduct of cinnamic acid and glycerin was obtained.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05426210uspto-grants-1995_06