반응 #50163
ord-0aba0da7a8164d719a0f863898cfe358
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1온도the mixture was heated
- 2온도to reflux for 12 hours
실험 절차
A solution of hexamethylenetretramine (1.87 mmol, 0.27 g) in trifluoroacetic acid (1.4 cm3) was added to benzo 15-crown-5 ether (1.87 mmol, 0.5 g) under nitrogen; the mixture was heated to reflux for 12 hours.