반응 #501446
ord-69a9ab89be9f4651bd0cf5bf0bbabf7f
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상세 조건
See reaction.notes.procedure_details.
실험 절차
In analogous fashion, 4-trifluoromethylaniline was reacted with t-butyl hypochlorite, ethyl 2-(methylthio)acetate and triethylamine followed by reduction of the 3-thiomethyl-5-trifluoromethyl-2-oxindole thus obtained with Raney nickel, to give 5-trifluoromethyl-2-oxindole, m.p. 189.5°-190.5° C.