반응 #499690
ord-cb5f92a66fae4325a924ce2b1426830e
반응 방정식
zirconium tetrachloride
titanium tetrachloride
methylene chloride
→
TiCl4 ZrCl4
반응 조건
상세 조건
See reaction.notes.procedure_details.
실험 절차
1.4 g (6.0 mmol) of zirconium tetrachloride and 10.207 g (53.8 mmol) of titanium tetrachloride were placed in a two-necked round-bottomed flask under an argon atmosphere. 480 ml of methylene chloride and 7 ml (7.89 g) of nitromethane were added (ratio Zr/nitro compound 1:21.5).