반응 #499689
ord-ca34c9294c9d49d8a9d2939565ec2598
반응 방정식
zirconium tetrachloride
aluminum trichloride
methylene chloride
→
AlCl3 ZrCl4
반응 조건
상세 조건
See reaction.notes.procedure_details.
실험 절차
0.7 g (3.0 mmol) of zirconium tetrachloride and 7.6 g (57.0 mmol) of aluminum trichloride were placed in a two-necked round-bottomed flask under an argon atmosphere. 480 ml of methylene chloride and 3 ml (3.38 g) of nitromethane were added (ratio Zr/nitro compound 1:18.4).