반응 #499688
ord-8b11187b3ec94ad888c5af91e5d386aa
반응 방정식
zirconium tetrachloride
aluminum trichloride
methylene chloride
→
AlCl3 ZrCl4
반응 조건
상세 조건
See reaction.notes.procedure_details.
실험 절차
1.2 g (5.1 mmol) of zirconium tetrachloride and 6.2 g (46.5 mmol) of aluminum trichloride were placed in a two-necked round-bottomed flask under an argon atmosphere. 410 ml of methylene chloride and 23 ml (25.9 g) of nitromethane were added (ratio Zr/nitro compound 1:82.5).