반응 #49932

반응 방정식

isonicotinyl chloride hydrochloride

N'-t-butyl-N'-benzoylhydrazine

sodium hydroxide

→

N'-t-butyl-N-isonicotinyl-N'-benzoylhydrazine

용매

toluene

반응 조건

후처리

1. 1
   기타The solids were removed by filtration
2. 2
   세척washed with water

실험 절차

A solution of N'-t-butyl-N'-benzoylhydrazine (0.5 g, 0.00026 mol) in 10 ml of toluene was treated with 50% sodium hydroxide (0.6 g) followed by isonicotinyl chloride hydrochloride (0.47 g, 0.0026 mol). The mixture was stirred at 23° C. overnight. The solids were removed by filtration and washed with water followed by ether to afford N'-t-butyl-N-isonicotinyl-N'-benzoylhydrazine.

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