반응 #49904

반응 방정식

N'-t-butyl-N-(thiobenzoyl)hydrazine

m-toluoyl chloride

toluene

→

N'-t-butyl-N-(thiobenzoyl)-N'-(3-toluoyl)hydrazine

용매

water

반응 조건

후처리

1. 1
   기타at 23° C
2. 2
   기타the product was isolated by filtration (0.25 g)

실험 절차

N'-t-butyl-N-(thiobenzoyl)hydrazine (ca. 1 g), m-toluoyl chloride (approx. 0.7 g) and 50% aqueous sodium hydroxide (6 drops) were mixed in 1 ml water and 10 ml toluene at 23° C. After stirring for 3 hours, ether-hexane was added and the product was isolated by filtration (0.25 g): m.p. 165°-168° C.

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