반응 #49902
ord-086b219308224dd4b83325a657c1c1e7
반응 방정식
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1여과filtered
실험 절차
The 1,1-dimethylethylhydrazine oxalate (2 g) was dissolved in toluene and neutralized with 50% aqueous sodium hydroxide. To this solution was added benzoyl chloride (4.02 g) and sodium hydroxide (50% Aq. solution) (2.45 g) at 25° C. The reaction mixture was warmed to room temperature and stirred 3 hours. The mixture was diluted with hexane and filtered to afford the product as a white solid (0.5 g).