반응 #498178

ord-5a18b1a3eb32402cb0d51adcaa7437dd

용매

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

N,N-Dibenzyl-N′-(2-fluoro-ethyl)ethane-1,2-diamine (160 mg) was prepared by following General Procedure S starting from dibenzyl-(2-chloro-ethyl)-amine (520 mg), 2-fluoro-ethylamine hydrochloride (250 mg), DIEA (900 uL) and tetrabutylammonium bromide (60 mg) in DMF (2 mL).

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US08759535B2uspto-grants-2014_06