반응 #49702

반응 방정식

4-n-Hexyloxybiphenyl carboxylic acid

thionyl chloride

→

4-n-hexyloxybiphenyl carboxylic acid chloride

반응 조건

후처리

1. 1
   온도under refluxing for 6 hours
2. 2
   workup.DISTILLATIONUnaltered thionyl chloride was distilled off

실험 절차

4-n-Hexyloxybiphenyl carboxylic acid (3.0 g) and an excessive amount of thionyl chloride were heated under refluxing for 6 hours. Unaltered thionyl chloride was distilled off to obtain 4-n-hexyloxybiphenyl carboxylic acid chloride.

출처