반응 #492956
ord-cda047e0ea6d438c932ab5e0b5713c40
용매
반응 조건
상세 조건
See reaction.notes.procedure_details.
실험 절차
6-Methylpicolinonitrile (12 mg, 0.1 mmol) was dissolved in EtOH (0.5 mL) and treated with NH2OH (1.5 eq of a 50% aq solution). The mixture was stirred at room temperature for 12 hours then reduced to dryness to afford N′-hydroxy-6-methylpicolinimidamide (6) as a clear yellow oil, which was used without purification.