반응 #4923
ord-c7bfc234f1744f32ad7ffb0232bfef78
반응 방정식
4-benzyl-2-(2-chloroethyl)-2,3-dihydro-1,4-benzoxazepin-5(4H)-one
dimethylamine
→
title compound
4-Benzyl-2-[2-(dimethylamino)ethyl]-2,3-dihydro-1,4-benzoxazepin-5(4H)-one monohydrate
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타were reacted
실험 절차
Following the procedure of Example 1, 4-benzyl-2-(2-chloroethyl)-2,3-dihydro-1,4-benzoxazepin-5(4H)-one and dimethylamine were reacted and the free base of the title compound was obtained in the concentrated residue. Recrystallization from ethanol-water gave the product, m.p. 75°-77° C.