반응 #488145

ord-f50b9c98d4654749a96f56fe5f9a14ef

반응 방정식

CC(C)(C)c1nc(Cl)c2nnn(Cc3ccccc3Cl)c2n1
5-tert-butyl-7-chloro-3-(2-chlorobenzyl)-3H-[1,2,3]triazolo[4,5-d]pyrimidine
COC(=O)C1CNC1
methyl azetidine-3-carboxylate
CC(C)(C)c1nc(N2CCOCC2)c2nnn(Cc3ccccc3Cl)c2n1
5-tert-butyl-3-(2-chlorobenzyl)-7-morpholin-4-yl-3H-[1,2,3]triazolo[4,5-d]pyrimidine
CC(C)(C)c1nc(N2CCOCC2)c2nnn(Cc3ccccc3Cl)c2n1
5-tert-Butyl-3-(2-chloro-benzyl)-7-morpholin-4-yl-3H-[1,2,3]triazolo[4,5-d]pyrimidine
COC(=O)C1CN(c2nc(C(C)(C)C)nc3c2nnn3Cc2ccccc2Cl)C1
title compound
COC(=O)C1CN(c2nc(C(C)(C)C)nc3c2nnn3Cc2ccccc2Cl)C1
1-[5-tert-Butyl-3-(2-chloro-benzyl)-3H-[1,2,3]triazolo[4,5-d]pyrimidin-7-yl]-azetidine-3-carboxylic acid methyl ester

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

In analogy to the procedure described for the synthesis of 5-tert-butyl-3-(2-chlorobenzyl)-7-morpholin-4-yl-3H-[1,2,3]triazolo[4,5-d]pyrimidine (example 1, step c), the title compound was prepared from 5-tert-butyl-7-chloro-3-(2-chlorobenzyl)-3H-[1,2,3]triazolo[4,5-d]pyrimidine and methyl azetidine-3-carboxylate. MS (m/e): 415.3 (MH+).

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US08741906B2uspto-grants-2014_06