반응 #486774

ord-c98b7673800c423ab70c75f3ebae4e4f

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    여과the product filtered off
  2. 2
    세척washed with dichloromethane

실험 절차

1-Benzyl-1-(cyanoacetyl)-3-[3-(methoxycarbonyl)phenyl]urea (3.51 g) was dissolved in dichloromethane (50 ml) and triethylamine (1.52 g) added. The mixture was stirred for one hour at room temperature and the product filtered off and washed with dichloromethane. Yield=3.16 g.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05821366uspto-grants-1998_10