반응 #485108
ord-4762e548988d4e4cbd7a105b68abb611
반응 방정식
반응물
시약
반응 조건
상세 조건
See reaction.notes.procedure_details.
실험 절차
Following the general method described in example 234, 3-(methylthio)aniline was reacted with triethyl orthoformate, ethyl nitroacetate and acetic acid followed by treatment with triethyl orthoformate, iron and acetic acid and subsequent alkaline hydrolysis. The title compound was obtained as a grey crystalline solid. Mp. 190-192° C. (H2O/dioxane), MS: m/e=234 (M+).