반응 #48109
ord-087999f7e0d549caa6d74fe79b97b3d8
반응 조건
상세 조건
See reaction.notes.procedure_details.
실험 절차
In a departure from the procedure described above the compound is prepared from 4-difluoromethyl-1-iodo-benzene (prepared from 4-iodobenzaldehyde using diethylaminosulfurtrifluoride (DAST) in dichloromethane) using iPrMgCl to generate the arylmetal compound and trapping this intermediate with trimethyl borate.