반응 #479702
ord-9909a9a5f8c54061893a864b5514024b
반응 방정식
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타was closed
- 2기타A precipitated solid was dried under reduced pressure at 80° C. for 24 hours
실험 절차
50 mL of Catalyst B, 40.0 g of stearyl glycidyl ether (SGE) and 22.8 g of octyl glycidyl ether (OGE) were added to 210 ml of toluene, and a vessel was closed. The polymerization was carried out at 130° C. for 24 hours with stirring. The reaction solution was added to a large amount of acetone containing a small amount of a dilute solution of hydrogen chloride. A precipitated solid was dried under reduced pressure at 80° C. for 24 hours to obtain a poly(stearyl glycidyl ether/octyl glycidyl ether) copolymer. Pale yellow solid. Yield 75%.