반응 #475066

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3-Methylthiopropylamine

hexane ethyl acetate

→

title compound

수율 93.1%

Phenyl N-(3-methylthiopropyl)carbamate

수율 93.1%

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실험 절차

3-Methylthiopropylamine (5.5 ml, 50 mmol) was used for reaction in the same manner as Production Example 310-1, and purification was performed by silica gel column chromatography (hexane/ethyl acetate system) to obtain the title compound (10.486 g, 46.54 mmol, 93.08%) as a yellow oil.

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