반응 #474594

ord-552e1eb460184a13962895d2a98a30b6

용매

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타reaction temperature, 80° C.
  2. 2
    기타reaction time, 2 hours
  3. 3
    기타yield

실험 절차

Benzyl azide (0.400 g, 3.00 mmol), diphenylacetylene (0.588 g, 3.30 mmol), Cp*RuCl(PPh3)2 (25 mg, 0.031 mmol). Solvent, benzene; reaction temperature, 80° C.; reaction time, 2 hours; yield, 0.75 g (80%). EI-MS: m/z 312 [M+1].

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US08372986B2uspto-grants-2013_02